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Qualitative & Quantitative Analyzer

HPLC+GC-MS Triple analyzer, GC-MS, LC-MS, IC, FTIR, XRD, UV/Vis Spectrometer

XRD-3000 X-ray Diffraction

Technical parameter

Model No.

XRD-3000

Rated power

3kW

Tube voltage

10-60kV

Tube current

5-80mA

X-ray tube

Glass tube, ceramic tube, ripple ceramic tube: Cu, Fe, Co, Cr, Mo etc, Power 2kW

Focus size

1 x 10mm or 0.4 x14mm or 2 x 12mm

Stability

≤0.01%

Goniometer structure

Horizontal (θ -2θ)

Radius of diffraction

185mm

Scanning range

0-164

Scanning speed

0.0012° – 70° min

Max. revolving speed

100°/min

Scanning fashion

θ -2θ linkage, θ 、2θ single action; continuous or stepping scanning

Angle repeatable accuracy

1/1000°

Minimal stepping angle

1/1000°

Detector

Proportional counters (PC) or scintillation counters (SC)

Maximal  counting rate of linearity

5x105 CPS (with the compensate function of drop out counting)

Energy resolution ratio

≤25% (PC), ≤50% (SC)

Counting fashion

Differential coefficient or integral, PHA automatically, dead time regulate

Stability of system measure

≤0.01%

Scattered rays dose

≤1μ Sv/h (without X-ray protective device)

Instrument integrative stability

≤0.5%

Dimension

1100 x 850 x1750mm

 

XRD-3000 X-Ray Diffractometer Components 

X-Ray High Voltage Generator

  1. 1505 High Voltage Transformer   
  2. AL-75kV High Voltage Cable 
  3. 9850 Control panel  
  4. 9820 High voltage control unit
  5. 9830 Control gate
  6. 9810 System Case
  7. 9840 Main power cable
  8. X-ray tube 2kW Cu, Focus size 1×10mm²
  9. 3306 Tube holder
  10. 9924 X-ray Protective cover

 

  Angle Measuring System

  1. 3501 Goniometer    
  2. Goniometer layer board
  3. Powder sample holder  
  4. Powder sample plate with blind Holes
  5. Powder sample plate with through holes
  6. Micronutrient powder sample board
  7. Zero setting sample piece, double-knife edge slit
  8. Standard ruler, watch oil
  9. Filter Ni   
  10. Slit

 

Recording and Controlling Unit

  1. 2013 Recording and controlling units  
  2. CH132 Scintillation counter
  3. Counter cable
  4. Stepping motor cable
  5. Interface cable

 

Circulating Water Cooling System

  1. ZFB-3000 Cooling device
  2.  9509 Power cable   
  3.  Water pipe 6 meters
  4.  Water relay cable

 

Computer & System Control Program and Applicable Software

  1. Data collecting and processing software
  2. Data analysis and processing software  
  3. Application software    
  4. Diffraction data card stock

 

Technical Material

  1. XRD-3000 X-ray diffractometer user manual
  2. ZFB-3000 Cooling device user manual

 

Spare Parts

  1. Ring rubber blanket
  2. Fuse 2A, 3A, 6A

 

X-Ray Diffractometer Property and Technical Parameter

 High pressure generatorAdopting imported PLC control technology

  • Rated Power:3kW
  • Tube Voltage:10~60kV  It is automatically controlled by computer terminal(1kV/step)
  • Tube Current:5~80mA  It is automatically controlled by computer terminal(1mA/step)
  • Tube Voltage and Current Stability≤0.01%
  • Protection of over voltage, over current, over power, and low water level
  • X-Ray Tube:Cu target、Focal point 1×10mm2、Power 2.0kW;
  • Optical shutter switch is automatically controlled by computer terminal
  • Unibody structure cooling device, Cooling device is unibody structure, and the automatic temperature control system can indicate the water temperature of X-ray tube.

It adopts PLC control technology, has high degree of automation, low failure rate, strong anti-jamming capability, excellent system stability and long using life.

 

Goniometer and Control (Horizontal type):

Horizontal Type θ -2θ, diffraction circle radius 185mm; Rotation of goniometer is controlled by stepping motor (forward or reverse, forward scan),  drive mode (move individually or jointly ), scanning mode(continuous, stepping), scanning speed, it can do angle-auto correction, detect losing step and avoid lost motion;  

  • Minimum Step Angle: 0.001°
  • Continues Scan Speed: 0.0012°-70°min
  • Step scanning step width angle: 0.005~165°
  • 2θ Angle measurement range:≤0.005°
  • 2θ Angle measurement range:0--164°
  • Goniometer 2θ angle uni-directional Repeatability 0.001°

 

Recording and Controlling Unit and Detector:

  • Closed scintillation counter
  • Auto differential and integral conversion
  • Base line and channel width: 0%~99%
  • Continuous adjustable high voltage of detector : 0~2000V
  • High voltage stability of detector: ≤0.01%
  • Optional X-ray tube target material: Cr、Fe、Co、Cu、Mo
  • Energy Spectrum Analysis (Cu,Kα CuKa Curve): ≤25% (PC), ≤50% (SC)

 

Overall Stability

System overall stability ≤0.3%

 

Outline Dimension

Outline Dimension:1100×850×1750mm

XRD-3000 X-ray Diffraction 


 

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